Abstract:The nonylphenol molecularly imprinted materials was prepared by combining molecular imprinting technique with a sol-gel process. In this process, nonylphenol was applied as the template, 3-aminopropyltriethoxysilane as function monomer, tetracethoxysilicane as cross linker. The performance of the materials was also studied. The results show that the material is promising for selective separation and removal of nonylphenol from environmental samples.